Failure Analysis

I spent part of the day working on a failure analysis of a high-pressure pump head used in one of the instruments I helped to design for a client. I am fairly confident that I have determined the root cause of the failure and these photos will be part of my report. A substance, which I have yet to identify, is accumulating on the glass piston rod and mating high-pressure seal which increases the friction between these components enough to prevent normal piston motion.